Reaktion #83728

ord-dfbe1e82b8724e8cba9ff2d90af96eb8

Reaktionsgleichung

O=C(c1ccc(O)cc1)c1cc(Cl)ccc1Cl
4'-Hydroxy-2,5-dichlorobenzophenone
Oc1ccccc1
phenol
O=C(Cl)c1cc(Cl)ccc1Cl
2,5-dichlorobenzoyl-chloride
CC(=O)Cl
acetyl chloride
→
CC(=O)Oc1ccc(C(=O)c2cc(Cl)ccc2Cl)cc1
4'-Acetoxy-2,5-dichlorobenzophenone

Edukte

O=C(c1ccc(O)cc1)c1cc(Cl)ccc1Cl
4'-Hydroxy-2,5-dichlorobenzophenone
Oc1ccccc1
phenol
O=C(Cl)c1cc(Cl)ccc1Cl
2,5-dichlorobenzoyl-chloride
CC(=O)Cl
acetyl chloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

4'-Acetoxy-2,5-dichlorobenzophenone is prepared by treating 4'-Hydroxy-2,5-dichlorobenzophenone, which is prepared by the Friedel-Crafts acylation of phenol with 2,5-dichlorobenzoyl-chloride, with acetyl chloride.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05625010uspto-grants-1997_04