Reaktion #833512

Reaktionsgleichung

Ethyl vanillin

allyl bromide

potassium carbonate

→

3-ethoxy-4-(2-propenyloxy)benzaldehyde

Lösungsmittel

acetone

Reaktionsbedingungen

Aufarbeitung

1. 1
   TemperaturAfter cooling
2. 2
   Filtrationthe solid was filtered off
3. 3
   Waschenwashed with acetone
4. 4
   SonstigeA yellow oil was obtained
5. 5
   Einengenafter a thorough concentration of the organic phases

Vorschrift

Ethyl vanillin (21.6 g, 0.130 mol) and allyl bromide (19.9 g, 0.160 mol) were heated under reflux together with potassium carbonate (27.3 g, 0.200 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. A yellow oil was obtained after a thorough concentration of the organic phases.

Quelle