Reaktion #83350

Reaktionsgleichung

4-(4-aminophenylthio)-7-trifluoromethylquinoline

4-chloro-3-trifluoromethylphenylisothiocyanate

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title compound

Ausbeute 63.0%

1-[4-(7-Trifluoromethyl-4-quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea

Ausbeute 63.0%

Reaktionsbedingungen

Vorschrift

4-(4-aminophenylthio)-7-trifluoromethylquinoline (0.01 mole, 3.2 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (0.01 mole, 2.4 g) were reacted according to procedure C to yield the title compound 3.5 g, 63%. Mass Spec (FD) 557. Calculated for C24H14ClF6N3S2 : C, 51.66; H, 2.53; N, 7.53. Found: C, 51.92; H, 2.53; N, 7.46.

Quelle