Reaktion #83347

Reaktionsgleichung

4-(4-aminophenylthio)quinoline

4-chloro-3-trifluoromethylphenylisothiocyanate

→

title compound

Ausbeute 56.0%

1-[4-(4-Quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea

Ausbeute 56.0%

Reaktionsbedingungen

Vorschrift

4-(4-aminophenylthio)quinoline (3.9 moles, 1.0 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (3.9 moles, 0.92 g) were reacted according to procedure A to yield of the title compound 1.06 g, 56%. Mass spec (FD) 490. Calculated for C23H15ClF3N3S2 : C, 56.38; H, 3.09, N, 8.58. Found: C, 56.60; H, 3.11; N, 8.42.

Quelle