Reaktion #83081

Reaktionsgleichung

p-nitrobenzyl chloroformate

p-nitrophenol

triethylamine

→

desired product

Ausbeute 37.1%

Carbonic acid 4-Nitrophenyl (4-Nitrophenyl)methyl Ester

Ausbeute 37.1%

Lösungsmittel

tetrahydrofuran

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe formed solid is collected
2. 2
   Waschenwashed with water
3. 3
   Sonstigedried

Vorschrift

To an ice cooled solution, under argon, of 7.3 g of p-nitrophenol and 7.5 ml of triethylamine in 36 ml of dry tetrahydrofuran, is added, dropwise, a solution of 10.78 g of p-nitrobenzyl chloroformate in 18 ml of dry tetraydrofuran. The reaction mixture, a suspension, is stirred at room temperature overnight. The formed solid is collected, washed with water and dried to give 5.9 g of the desired product.

Quelle