Reaktion #828717

ord-124348c9e3c74a01bcdfa140f15247e0

Reagenzien

Keine

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeAfter the completion of the reaction
  2. 2
    SonstigeAfter separating the lower layer from the upper layer
  3. 3
    Sonstigeto obtain D-HPAE, which

Vorschrift

After the completion of the reaction, an extractant such as ethyl acetate is added to the reaction mixture which separates the reaction mixture into an upper layer and a lower layer. The upper layer contains D-HPAE in the organic solvent and the lower layer contains L-HPA in water. After separating the lower layer from the upper layer, the extractant, i.e., ethyl acetate, can be vaporized to obtain D-HPAE, which can be chemically hydrolyzed to obtain D-homophenylalanine.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05552317uspto-grants-1996_09