Reaktion #822559

ord-c9b6ceaffd874fe3ad546c63aa66dd6b

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigea pale yellow solid is obtained (0.05 g; yield=23%; m.p.=166° C.)

Vorschrift

In a manner similar to that of Example 1 g, by reacting 0.23 g (0.5 mmol) of methyl 5-(8,8-dimethyl-5-p-tolyl-7,8-dihydro-2-naphthylselanyl)-3-methylpent-2-en-4-ynoate with 0.23 g (5.5 mmol) of lithium hydroxide monohydrate, a pale yellow solid is obtained (0.05 g; yield=23%; m.p.=166° C.).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07592478B2uspto-grants-2009_09