Reaktion #821955

Reaktionsgleichung

1-benzyl-4-methylpyridinium chloride

EtOAc MeOH NH3

→

1-benzyl-4-methyl-1,2,3,6-tetrahydropyridine

Reaktionsbedingungen

Vorschrift

The product was obtained analogously to IP 5b starting from 10.0 g (45.5 mmol) of 1-benzyl-4-methylpyridinium chloride. Yield: 7.15 g (84% of theoretical); C13H17N (M=187.281); calc.: molpeak (M+H)+: 188; found: molpeak (M+H)+: 188; Rf value: 0.95 (silica gel, EtOAc/MeOH/NH3 9:1:0.1).

Quelle