Reaktion #82144

Reaktionsgleichung

tartaric acid

→

Cis-Epoxysuccinic Acid

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe polymer was filtered
2. 2
   ExtraktionThe ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor
3. 3
   Sonstigedried
4. 4
   Sonstigeto afford a pale brown solid which

Vorschrift

The resulting heterogeneous reaction mixture, which was lumpy and hardened, was neutralized by addition of 15% aqueous tartaric acid solution. The polymer was filtered and a small portion was ground thoroughly. The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor and dried to afford a pale brown solid which was not soluble to any extent in distilled water.

Quelle