Reaktion #81583

ord-55377aaf0cc146dfad2fb4f30a07c2d6

Reaktionsgleichung

CCOC(=O)Cc1ccc(Br)cc1
ethyl (4-bromophenyl)acetate
CCOC(=O)Cc1ccc(Br)cc1
Compound A
CCOC(=O)Cc1ccc(Br)cc1
ethyl (4-bromophenyl)acetate
O=C(O)Cc1cccc(Br)c1
3-bromophenylacetic acid
CCOC(=O)Cc1cccc(Br)c1
title compound
CCOC(=O)Cc1cccc(Br)c1
Ethyl (3-bromophenyl)acetate

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Employing the same general procedure as for the preparation of ethyl (4-bromophenyl)acetate (Compound A), 100 g (463 mmol) of 3-bromophenylacetic acid was converted into the title compound (yellow oil) using 2 g of conc. H2SO4 and 500 ml of ethanol.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05618943uspto-grants-1997_04