Reaktion #81236

Reaktionsgleichung

phthalidyl 4-(1-hydroxy-1-methylethyl)-2-propylimidazole-5-carboxylate

4-[2-(trityltetrazol-5-yl)phenyl]benzyl bromide

potassium carbonate

→

title compound

Ausbeute 18.1%

Phthalidyl 4-(1-hydroxy-1-methylethyl)-2-propyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate

Ausbeute 18.1%

Reaktionsbedingungen

Vorschrift

Following a procedure similar to that described in Example 61(a), but using 0.456 g of phthalidyl 4-(1-hydroxy-1-methylethyl)-2-propylimidazole-5-carboxylate (prepared as described in Preparation 32), 0.736 g of 4-[2-(trityltetrazol-5-yl)phenyl]benzyl bromide and 0.366 g of potassium carbonate, 0.196 g of the title compound was obtained, melting at 118°-120° C.

Quelle