Reaktion #806368

Reaktionsgleichung

10-fluoro-4-methoxy-benzo[a]phenazine-11-carboxylic acid methyl ester

methylamine

→

crude desired title compound

4-Methoxy-10-methylamino-benzo[a]phenazine-11-carboxylic acid methyl ester

Lösungsmittel

tetrahydrofuran

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe solvent was then removed in vacuo

Vorschrift

A mixture of 10-fluoro-4-methoxy-benzo[a]phenazine-11-carboxylic acid methyl ester (IV.5) (100 mg) and 2.0M solution of methylamine in tetrahydrofuran was stirred at room temperature for 18 hours. The solvent was then removed in vacuo to yield the crude desired title compound as an orange solid.

Quelle