Reaktion #80567

Reaktionsgleichung

cyclobutanecarbonyl chloride

N-[2-(1-naphthyl)ethyl]amine hydrochloride

potassium carbonate

→

N-[2-(1-naphthyl)ethyl]cyclobutanecarboxamide

Lösungsmittel

water chloroform

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONis then added with magnetic stirring
2. 2
   TemperaturThe reaction mixture is cooled in an ice bath

Vorschrift

0.01 mol of N-[2-(1-naphthyl)ethyl]amine hydrochloride is dissolved in a water/chloroform (40: 60; vol/vol ) mixture, and 0.02 mol of potassium carbonate is then added with magnetic stirring. The reaction mixture is cooled in an ice bath, and 0.01 mol of cyclobutanecarbonyl chloride is then added dropwise with magnetic stirring.

Quelle