Reaktion #803613

ord-f2651ff79f8b485785e6afc1ce418be4

Reaktionsgleichung

O=C[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO
glucose
Cc1ncc(C[n+]2csc(CCO)c2C)c(N)n1.Cl.[Cl-]
thiamine hydrochloride
O=P([O-])(O)O.[K+]
potassium dihydrogenphosphate
O=C([O-])[O-].[Ca+2]
calcium carbonate
NC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O[C@H]3O[C@H](CO)[C@@H](O)[C@H](N)[C@H]3O)[C@H](N)C[C@@H]2N)[C@H](O)[C@@H](O)[C@@H]1O
kanamycin
O.O.O.O.O.O.O.O=S(=O)([O-])[O-].[Mg+2]
magnesium sulfate heptahydrate
CCOc1ccc(Nc2ccc(C(=C3C=CC(=[N+](CC)Cc4cccc(S(=O)(=O)[O-])c4)C=C3)c3ccc(N(CC)Cc4cccc(S(=O)(=O)[O-])c4)cc3)cc2)cc1.[Na+]
CBB R250
CCCCCCCCCCCCOS(=O)(=O)[O-].[Na+]
SDS
O=S(=O)([O-])[O-].[NH4+].[NH4+]
ammonium sulfate
O=C(O)CCCC[C@@H]1SC[C@@H]2NC(=O)N[C@@H]21
biotin
CSCCC(N)C(=O)O
DL-methionine
CC1(C)S[C@@H]2[C@H](NC(=O)Cc3ccccc3)C(=O)N2[C@H]1C(=O)[O-].[K+]
Penicillin

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeAfter completion of the culture, culture supernatant obtained

Vorschrift

The secretory expression system of the protransglutaminase using C. glutamicum has already been reported (WO01/23591). Then, by using the plasmid vector pPKSPTG1 for secretory expression of protransglutaminase described in WO01/23591, each of the YDK010 strain and the YDK010ΔPBP1a strain was transformed. Each of the obtained transformants was cultured in the MM liquid medium (120 g of glucose, 3 g of magnesium sulfate heptahydrate, 30 g of ammonium sulfate, 1.5 g of potassium dihydrogenphosphate, 0.03 g of iron sulfate heptahydrate, 0.03 g of manganese sulfate pentahydrate, 450 μg of thiamine hydrochloride, 450 μg of biotin, 0.15 g of DL-methionine, and 50 g of calcium carbonate in a volume of 1 L with water, adjusted to pH 7.0) containing 25 mg/l of kanamycin at 30° C. for 72 hours. After completion of the culture, culture supernatant obtained by centrifuging each culture broth was subjected to reduced SDS-PAGE, and then stained with CBB R250 (produced by Bio-Rad). Secretion amounts of the protransglutaminase were determined according to the previous report (Protein Expr. Purif., 26:329-335), and the amounts were compared. As a result, the secretion amount of the protransglutaminase was significantly improved in the YDK010ΔPBP1a strain compared with that observed for the parent strain YDK010 (FIG. 8).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09187554B2uspto-grants-2015_11