Reaktion #80360

ord-d6eb3ccc027f4a8ebbe76dcd095d4b01

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Following a procedure similar to that described in Example 33, but using N-[4-(4-piperidinomethyl-2-pyridyloxy) -cis-2-butenyl]-2-chloroacetamide (prepared as described in Preparation 1) and 3-mercapto-1,2,4-triazole as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as a white powder, melting at 65°-67° C., in a 91% yield.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05616579uspto-grants-1997_04