Reaktion #799022

Reaktionsgleichung

3-amino-2,2-dimethylpropan-1-ol

ethyl isocyanate

→

title compound

Ausbeute 100.0%

1-ethyl-3-(3-hydroxy-2,2-dimethylpropyl)urea

Ausbeute 100.0%

Lösungsmittel

1,4-dioxane

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe solvent was removed under reduced pressure

Vorschrift

To a solution of 3-amino-2,2-dimethylpropan-1-ol (1.03 g, 10 mmol) in dry 1,4-dioxane (20 mL) was added dropwise ethyl isocyanate (0.71 g, 10 mmol) at room temperature under nitrogen. The reaction mixture was then stirred at room temperature under nitrogen overnight. The solvent was removed under reduced pressure to give the title compound as colorless oil (1.74 g, 100%). MS 175 (MH+).

Quelle