Reaktion #78804

ord-51cf999c4b4c4eb2807f6b59daff936c

Reaktionsgleichung

O=COC1CC2C=CC1C2
5-norbomene-2-yl formate
C=CC=O
acrolein
O=COC1CC2CC1C1OC=CCC21
3-oxa-tricyclo[6.2.1.02,7]undec-4-ene-10-yl formate
Ausbeute 49.0%

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigesynthesize

Vorschrift

248 g of 5-norbomene-2-yl formate and 33.6 g of acrolein were reacted in the same manner asin Examplel1-1to synthesize adesired product. As aresult, 57 g of 3-oxa-tricyclo[6.2.1.02,7]undec-4-ene-10-yl formate was obtained.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06713228B2uspto-grants-2004_03