Reaktion #78410

Reaktionsgleichung

acrylate

cyclopentadiene

toluene

→

Dicyclopentadiene

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe derivative was synthesized
2. 2
   Temperaturcooled with ice

Vorschrift

The derivative was synthesized as follows. 20 grams of the derivative of acrylate obtained as the third example was dissolved in 20 milliliters of toluene. 7 grams of cyclopentadiene was dropped into the solution cooled with ice, and was agitated through all night. Dicyclopentadiene was produced as by-product, and was eliminated in vacuum. Then, 24.9 grams of the derivative of norbornene was obtained. The derivative of norbornene was viscous liquid, and the yield was 95%.

Quelle