Reaktion #77221

ord-13eb5773655d4e50838db3d487030975

Reaktionsgleichung

C#Cc1cccc(C)c1
1-ethynyl-3-methyl-benzene
CCOC(=O)c1c(C)nc(Br)n1C
2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester
→
CCOC(=O)c1c(C)nc(C#Cc2cccc(C)c2)n1C
title compound
CCOC(=O)c1c(C)nc(C#Cc2cccc(C)c2)n1C
3,5-Dimethyl-2-m-tolylethynyl-3H-imidazole-4-carboxylic acid ethyl ester

Edukte

C#Cc1cccc(C)c1
1-ethynyl-3-methyl-benzene
CCOC(=O)c1c(C)nc(Br)n1C
2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound, MS: m/e=283.6 (M+H+), was prepared in accordance with the general method of example 1b from 1-ethynyl-3-methyl-benzene and 2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06706707B2uspto-grants-2004_03