Reaktion #76686

Reaktionsgleichung

2-chloro-1-thia-2,3,5,7-tetraazaindene

2-aminoindan

→

title compound

Ausbeute 51.7%

2-(2-Indanylamino)-1-thia-2,3,5,7-tetraazaindene

Ausbeute 51.7%

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe product obtained
2. 2
   Sonstigewas purified by silica gel chromatography (hexane:ethyl acetate=3:1)

Vorschrift

Using 2-chloro-1-thia-2,3,5,7-tetraazaindene (50 mg, 0.29 mmol) (see J. Org. Chem. 26, 4961 (1961), J. Chem. Soc. (C) 1856 (1967)) and 2-aminoindan (120 mg, 0.90 mmol), a similar procedure to Production Example 190 was carried out. The product obtained was purified by silica gel chromatography (hexane:ethyl acetate=3:1) to obtain the title compound (41 mg, 0.15 mmol) having the following physical properties:

Quelle