Reaktion #76491

ord-7254d1bc18134c949e814f0cd113c64c

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

A solution of 5-amino-6-nitroquinoline (25 g, 0.13 mol) in THF (500 mL) and methanol (500 mL) was treated with Raney nickel (7 g) under a hydrogen atmosphere (50.4 psi) on a Parr apparatus for 3.4 hours. Standard work-up gave the 5,6-diaminoquinoline.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06703391B2uspto-grants-2004_03