Reaktion #76462

Reaktionsgleichung

2,6-dichloro-9-isopropylpurine

benzylamine

→

6-benzylamino-2-chloro-9-isopropylpurine

Ausbeute 85.0%

Lösungsmittel

n-butanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe reaction mixture (after evaporation of n-butanol)

Vorschrift

2,6-dichloro-9-isopropylpurine (1 mmol) and benzylamine (3.5 mmol) were heated with stirring in 3 ml of n-butanol (3 hour, 110° C.). The reaction mixture (after evaporation of n-butanol) was worked up as above for the compound 2, yield 85-90%.

Quelle