Reaktion #75699

ord-4fac8855370d4f90a74b316a3e19cc3c

Reaktionsgleichung

CCC(C)c1ccc(N)cc1
4-sec-butylaniline
CCOC(=O)C=O
glyoxylic acid ethyl ester
C=Cc1cc2c(cc1Cl)OCO2
5-chloro-6-vinyl-benzo[1,3]dioxol
→
CCOC(=O)C1CC(c2cc3c(cc2Cl)OCO3)c2cc(C(C)CC)ccc2N1
Compound 77
CCOC(=O)C1CC(c2cc3c(cc2Cl)OCO3)c2cc(C(C)CC)ccc2N1
6-sec-butyl-4-(6-chlorobenzo[1,3]dioxol-5-yl)-1,2,3,4-tetrahydroquinoline-2-carboxylic Acid Ethyl Ester

Edukte

CCC(C)c1ccc(N)cc1
4-sec-butylaniline
CCOC(=O)C=O
glyoxylic acid ethyl ester
C=Cc1cc2c(cc1Cl)OCO2
5-chloro-6-vinyl-benzo[1,3]dioxol

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Compound 77 was prepared from 4-sec-butylaniline, glyoxylic acid ethyl ester and 5-chloro-6-vinyl-benzo[1,3]dioxol by the automated process.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06699877B2uspto-grants-2004_03