Reaktion #75693

ord-eb3b5948b8064207bc191357b8dc9e1b

Reaktionsgleichung

Nc1cc(Cl)c(Cl)cc1Cl
2,4,5-trichloroaniline
O=CC(=O)O
glyoxylic acid
C1=COCC1
2,3-dihydrofuran
→
O=C(O)C1Nc2c(Cl)cc(Cl)c(Cl)c2C2OCCC12
Compound 67
O=C(O)C1Nc2c(Cl)cc(Cl)c(Cl)c2C2OCCC12
6,8,9-trichloro-2,3,3a,4,5,9b-hexahydro-furo[3,2-c]quinoline-4-carboxylic Acid

Edukte

Nc1cc(Cl)c(Cl)cc1Cl
2,4,5-trichloroaniline
O=CC(=O)O
glyoxylic acid
C1=COCC1
2,3-dihydrofuran

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Compound 67 was prepared from 2,4,5-trichloroaniline, glyoxylic acid and 2,3-dihydrofuran by the automated process.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06699877B2uspto-grants-2004_03