Reaktion #75691

Reaktionsgleichung

3,5-dichloroaniline

ethylglyoxalate

indene

trifluoroacetic acid

→

Compound 61

Ausbeute 89.0%

5,6a,7,11b-tetrahydro-6H-indeno-[2, 1-c]quinoline-6-carboxylic Acid Ethyl Ester

Ausbeute 89.0%

Lösungsmittel

acetonitrile

Reaktionsbedingungen

Vorschrift

Compound 61 was prepared with a yield of 89% by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol indene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile.

Quelle