Reaktion #75669

Reaktionsgleichung

3,5-dichloroaniline

ethylglyoxalate

3-bromostyrene

trifluoroacetic acid

→

Compound 37

4-(3-bromophenyl)-5,7-dichloro-1,2,3,4-tetrahydroquinoline-2-carboxylic Acid Ethyl Ester

Lösungsmittel

acetonitrile

Reaktionsbedingungen

Vorschrift

Compound 37 was prepared by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol 3-bromostyrene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile.

Quelle