Reaktion #75647
ord-e8a931743b8149fd99a983cfe51a6d2b
Reaktionsgleichung
3,5-dichloroaniline
ethylglyoxalate
styrene
trifluoroacetic acid
→
Compound 14
5,7-dichloro-4-phenyl-1,2,3,4-tetrahydroquinoline-2-carboxylic Acid Ethyl Ester
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
Compound 14 was prepared by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol styrene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile.