Reaktion #75291

ord-3d92c6ce28bb4247ba978dfcc6f0040c

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe slightly exothermic reaction
  2. 2
    Sonstigewas accompanied by the precipitation of the solid N-phenacylpyridinium bromide
  3. 3
    FiltrationThe salt was then filtered
  4. 4
    Waschenwashed thoroughly with anhydrous ether

Vorschrift

N-phenacylpyridinium bromide was prepared by slowly adding phenacyl bromide to a stirred flask containing an equimolar quantity of pyridine. The slightly exothermic reaction was accompanied by the precipitation of the solid N-phenacylpyridinium bromide. The salt was then filtered and washed thoroughly with anhydrous ether.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04175973uspto-grants-1979_11