Reaktion #75291
ord-3d92c6ce28bb4247ba978dfcc6f0040c
Reaktionsgleichung
Edukte
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeThe slightly exothermic reaction
- 2Sonstigewas accompanied by the precipitation of the solid N-phenacylpyridinium bromide
- 3FiltrationThe salt was then filtered
- 4Waschenwashed thoroughly with anhydrous ether
Vorschrift
N-phenacylpyridinium bromide was prepared by slowly adding phenacyl bromide to a stirred flask containing an equimolar quantity of pyridine. The slightly exothermic reaction was accompanied by the precipitation of the solid N-phenacylpyridinium bromide. The salt was then filtered and washed thoroughly with anhydrous ether.