Reaktion #75031

ord-b8b0d7af08bb45c5b88e08b5a8efd0a7

Lösungsmittel

Reaktionsbedingungen

Temperatur
25°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeA 100-ml round-bottomed flask equipped with a magnetic stirrer
  2. 2
    SonstigeThe mixture formed

Vorschrift

A 100-ml round-bottomed flask equipped with a magnetic stirrer was charged with isobutyric anhydride (10 mmol), benzaldehyde (10 mmol), a mixture of alkanes (25 ml) having a boiling range of from 62° C. to 82° C., sodium cyanide (12 mmol) and water (3 ml). The mixture formed was stirred at a temperature of 25° C. The table presents the yields of the title ester after the reaction times indicated (Embodiment IV).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04175094uspto-grants-1979_11