Reaktion #75025
ord-e6f33265221e4ce2b908362c62e1a51c
Reaktionsgleichung
propionic acid
Octene-1
potassium propionate
→
alphamethyl-gamma-n-hexyl-butyrolactone
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
Octene-1 in an amount of 2.24 g. and 11.65 g. of manganic acetate, Mn(C2H3O2)3.2H2O, (comprising two equivalents of Mn+3 based on titration value), were refluxed under nitrogen in 200 ml. propionic acid containing 20 g. potassium propionate. In less than an hour a good yield of alphamethyl-gamma-n-hexyl-butyrolactone was obtained.