Reaktion #74893

ord-c5e415f74b814fec966c82cbe051672a

Reaktionsgleichung

CCC[CH2][Sn]([CH]1CCCCC1)([CH]1CCCCC1)[CH]1CCCCC1
butyl tricyclohexyltin
CCC[CH2][Sn]([Cl])([Cl])[Cl]
butyltin trichloride
→
[Cl][Sn]([CH]1CCCCC1)([CH]1CCCCC1)[CH]1CCCCC1
tricyclohexyltin chloride
CCC[CH2][Sn]([Cl])([Cl])[CH2]CCC
dibutyltin dichloride

Edukte

CCC[CH2][Sn]([CH]1CCCCC1)([CH]1CCCCC1)[CH]1CCCCC1
butyl tricyclohexyltin
CCC[CH2][Sn]([Cl])([Cl])[Cl]
butyltin trichloride

Reagenzien

Keine

Lösungsmittel

Cc1ccccc1C
xylene

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeAnalysis of the reaction mixture obtained

Vorschrift

A solution of equimolar amounts of butyl tricyclohexyltin and butyltin trichloride in commercial xylene was refluxed for 221/2 hours. Analysis of the reaction mixture obtained showed that the reaction had gone to about 89% completion to form predominantly tricyclohexyltin chloride and dibutyltin dichloride.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04174346uspto-grants-1979_11