Reaktion #74728

ord-3515206906a54475b5b70cde34b7c842

Reaktionsgleichung

Cc1cccc(Cl)c1Nc1ccccc1CC(=O)Oc1ccc([N+](=O)[O-])cc1
[o-(3-chloro-o-toluidino)-phenyl]-acetic acid-p-nitrophenyl ester
Cc1cccc(Cl)c1Nc1ccccc1CC(=O)O
[o-(3-chloro-o-toluidino)-phenyl]-acetic acid
→
O=C(Cc1ccccc1Nc1c(Cl)cccc1Cl)Oc1ccc([N+](=O)[O-])cc1
[o-(2,6-dichloroanilino)-phenyl]-acetic acid-p-nitrophenyl ester

Edukte

Cc1cccc(Cl)c1Nc1ccccc1CC(=O)Oc1ccc([N+](=O)[O-])cc1
[o-(3-chloro-o-toluidino)-phenyl]-acetic acid-p-nitrophenyl ester
Cc1cccc(Cl)c1Nc1ccccc1CC(=O)O
[o-(3-chloro-o-toluidino)-phenyl]-acetic acid
—
ether petroleum ether

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

[o-(3-chloro-o-toluidino)-phenyl]-acetic acid-p-nitrophenyl ester, starting with [o-(3-chloro-o-toluidino)-phenyl]-acetic acid, M.P. 124°-125° (from ether/petroleum ether).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04173577uspto-grants-1979_11