Reaktion #74686

Reaktionsgleichung

triphenylphosphine

chloromethyl ethyl ether

→

(Ethoxymethyl)triphenylphosphonium chloride

Lösungsmittel

benzene

Reaktionsbedingungen

Aufarbeitung

1. 1
   TemperaturThe mixture then was chilled
2. 2
   Filtrationfiltered
3. 3
   Sonstigeto give 7

Vorschrift

A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.

Quelle