Reaktion #744150

ord-f75907c016294692858f4de91dcc9f79

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    FiltrationThe mixture was filtered through kieselguhr
  2. 2
    Sonstigethe filtrate evaporated to dryness
  3. 3
    Sonstigeto give (1.31 g, 100%)

Vorschrift

Furo[2,3-c]pyridin-5-ylmethanol (1.29 g, 8.7 mmol) was dissolved in ethanol (50 ml) and hydrogenated at rt, 1 atmosphere over 10% palladium on charcoal paste for 18 h. The mixture was filtered through kieselguhr and the filtrate evaporated to dryness, to give (1.31 g, 100%).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08071592B2uspto-grants-2011_12