Reaktion #74327

ord-b68f555f13dd48f490f3332cb33d8177

Reaktionsgleichung

NC(=S)NCC1CCCCC1
N-(cyclohexylmethyl)thiourea
CCOC(=O)C(C)(C)Br
ethyl 2-bromoisobutyrate
→
CC1(C)SC(NCC2CCCCC2)=NC1=O
2-[(cyclohexylmethyl)amino]-5,5-dimethyl-1,3-thiazol-4(5H)-one

Edukte

NC(=S)NCC1CCCCC1
N-(cyclohexylmethyl)thiourea
CCOC(=O)C(C)(C)Br
ethyl 2-bromoisobutyrate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeSynthesis

Vorschrift

Synthesis was performed from N-(cyclohexylmethyl)thiourea and ethyl 2-bromoisobutyrate according to Method C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08541592B2uspto-grants-2013_09