Reaktion #742273

ord-b1dbd61695ec42a4809475f3bb8c1881

Reaktionsgleichung

O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(CC)CC
triethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(CC)CC
triethylamine
→
CC[NH+](CC)CC.O=S(=O)([O-])C(F)(F)F
triethylammonium trifluoromethanesulfonate

Edukte

O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(CC)CC
triethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(CC)CC
triethylamine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Temperaturwhile being cooled by liquid nitrogen
  2. 2
    Sonstigethus obtaining a target ionic conductor

Vorschrift

Equimolar amounts of triethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed triethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08071253B2uspto-grants-2011_12