Reaktion #740270

ord-a788334e0e47493e83b97cb24647815d

Reaktionsgleichung

OCCCCCCCCCCBr
10-bromodecanol
c1ccc(P(c2ccccc2)c2ccccc2)cc1
triphenylphosphine
→
OCCCCCCCCCC[P+](c1ccccc1)(c1ccccc1)c1ccccc1.[Br-]
10-Hydroxy-n-decyltriphenylphosphonium bromide

Edukte

OCCCCCCCCCCBr
10-bromodecanol
c1ccc(P(c2ccccc2)c2ccccc2)cc1
triphenylphosphine

Reagenzien

Keine

Lösungsmittel

CC#N
acetonitrile

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

A solution 10-bromodecanol (23.7 g) and triphenylphosphine (78.6 g) in dry acetonitrile (100 ml) was refluxed for 48 hours.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04675335uspto-grants-1987_06