Reaktion #738722

Reaktionsgleichung

tris(2-aminoethyl)amine

acrylate

HCl

→

TAEA acrylamide

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   Filtrationthe solid was filtered off
2. 2
   WaschenThe solid was then rinsed briefly with water twice
3. 3
   Trocknenisopropanol once, and dried in a vacuum oven
4. 4
   Sonstigeto yield 3.4 g

Vorschrift

Poly(NHS-acrylate) (4.4 g) was suspended in a solution containing water (100 mL) and tris(2-aminoethyl)amine (30 mL) which had been adjusted to pH 9 with concentrated HCl. After 4 days of stirring, the solid was filtered off, and the wash repeated. The solid was then rinsed briefly with water twice, isopropanol once, and dried in a vacuum oven to yield 3.4 g.

Quelle