Reaktion #737467

ord-46fce115f282424594cf5b4b4d132410

Reaktionsgleichung

c1ccc2c(c1)CC1OC21
2,3-epoxy-indane
CN1CCNCC1
N-methyl piperazine
CN1CCN(C2c3ccccc3CC2O)CC1
2,3-dihydro-1- (4- methyl-1-piperazinyl)-1H-inden-2-o1

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigewere reacted

Vorschrift

Using the procedure of Example 23, Step A, 14.57 g of 2,3-epoxy-indane and 12.4 ml of N-methyl piperazine were reacted to obtain 6.447 g of [trans (±)] 2,3-dihydro-1- (4- methyl-1-piperazinyl)-1H-inden-2-o1 melting at 132° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06271395B1uspto-grants-2001_08