Reaktion #7318

Reaktionsgleichung

trifluoromethanesulfonic anhydride

dimethyl carbonate

→

methyl trifluoromethanesulfonate

Ausbeute 197.7%

Reaktionsbedingungen

Vorschrift

731 g (2.59 mol) of trifluoromethanesulfonic anhydride and 232 g (2.58 mol) of dimethyl carbonate are added to the residue, and the process described above is repeated. 837 g of methyl trifluoromethanesulfonate having a purity of greater than 99% are isolated (yield: 99.1%).

Quelle