Reaktion #730461

Reaktionsgleichung

Methyl-6-bromo-2-naphtoate

lithiumaluminiumhydride

→

(6-Bromo-naphthalen-2-yl)-methanol

Lösungsmittel

tetrahydrofuran

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe crystalline product was recrystallized from ethanol (96%)

Vorschrift

Methyl-6-bromo-2-naphtoate (25 g, 94.3 mmol) was reduced with lithiumaluminiumhydride (5.36 g, 141.4 mmol) in tetrahydrofuran (200 ml). The crystalline product was recrystallized from ethanol (96%). Yield 15.84 g (70.8%).

Quelle