Reaktion #7289

Reaktionsgleichung

diethyl ether

2-methyl-2-adamantanol

acryloyl chloride

→

2-methyladamantyl acrylate

Ausbeute 55.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe reactant was reacted at room temperature for about 12 hours
2. 2
   Filtrationfiltered
3. 3
   SonstigeSubsequently, the solvent was removed by an evaporator
4. 4
   Sonstigethe reactant product was obtained
5. 5
   workup.DISTILLATIONvacuum distillation (yield: 55%)

Vorschrift

200 mL of diethyl ether was put into a round-neck flask, 41.5 g of 2-methyl-2-adamantanol and 27.6 g of tetraethyl amine were added thereto and then 22.6 g of acryloyl chloride was dropped. The reactant was reacted at room temperature for about 12 hours and then filtered using diethyl ether. Subsequently, the solvent was removed by an evaporator and then the reactant product was obtained using vacuum distillation (yield: 55%).

Quelle