Reaktion #72642

Reaktionsgleichung

N-(3-cyano-4,5-dimethylthiophen-2-ylcarbamoyl)benzamide

methyl iodide

→

2-Methoxy-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

Ausbeute 86.0%

Reaktionsbedingungen

Vorschrift

Prepared in a similar manner to Example 25 from N-(3-cyano-4,5-dimethylthiophen-2-ylcarbamoyl)benzamide (Example 4a) and methyl iodide in 86% yield. 1H NMR (400 MHz, CDCl3) δ2.35 (s, 3H), 2.36 (s, 3H), 3.53 (s, 3H), 6.0 (bs, 2H). MS 210 (MH+).

Quelle