Reaktion #72634

ord-02f3e18b5ac144fdb077f9105965bcb6

Reaktionsgleichung

CCNc1sc(C)c(C)c1C#N
2-(ethylamino)-4,5-dimethylthiophene-3-carbonitrile
O=C=NC(=O)c1ccccc1
benzoyl isocyanate
→
CCN(C(=O)NC(=O)c1ccccc1)c1sc(C)c(C)c1C#N
N-((3-Cyano-4,5-dimethylthiophen-2-yl)(ethyl)carbamoyl)benzamide

Edukte

CCNc1sc(C)c(C)c1C#N
2-(ethylamino)-4,5-dimethylthiophene-3-carbonitrile
O=C=NC(=O)c1ccccc1
benzoyl isocyanate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Prepared in a similar manner to Example 1a from 2-(ethylamino)-4,5-dimethylthiophene-3-carbonitrile (Example 21b) and benzoyl isocyanate. MS 328 (MH+).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08541421B2uspto-grants-2013_09