Reaktion #724202

Reaktionsgleichung

4-(1-(2-ethoxyethyl)-1H-benzimidazol-2-yl)[1,4]diazepane

hydriodic acid

→

title compound

4-(1-(2-Ethoxyethyl)-1H-benzimidazol-2-yl)[1,4]diazepane hydriodic Acid Salt

Lösungsmittel

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturcool
2. 2
   Sonstigeto give a solid
3. 3
   SonstigeCollect the solid
4. 4
   Filtrationby filtration
5. 5
   Waschenrinse with diethyl ether
6. 6
   Sonstigedry in vacuo

Vorschrift

Alternately, combine 4-(1-(2-ethoxyethyl)-1H-benzimidazol-2-yl)[1,4]diazepane (18.42 g, 63.9 mmol), 57% hydriodic acid (8.30 mL), ethanol (80 mL) and stir. After 2.5 hours, cool to give a solid. Collect the solid by filtration, rinse with diethyl ether, and dry in vacuo to give the title compound.

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