Reaktion #722648

Reaktionsgleichung

2-acetamido-2-(2-(2-benzyloxyphenyl)ethyl)pentyl acetate

→

compound

Ausbeute 93.4%

2-Acetamido-2-(2-(2-hydroxyphenyl)ethyl)pentyl acetate

Ausbeute 93.4%

Lösungsmittel

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationCatalyst was filtered off from the reaction solution
2. 2
   workup.DISTILLATIONthe solvent was distilled away under reduced pressure

Vorschrift

To a solution of 2-acetamido-2-(2-(2-benzyloxyphenyl)ethyl)pentyl acetate (0.90 g) in ethanol (45 ml), 10% palladium-carbon (0.40 g) was added and the mixture was subjected to catalytic reduction at room temperature for 6 hours. Catalyst was filtered off from the reaction solution and the solvent was distilled away under reduced pressure to give the subject compound (0.65 g).

Quelle