Reaktion #721789

Reaktionsgleichung

1-methylimidazole

octadecyl p-toluenesulfonate

→

title compound

Ausbeute 91.3%

1-methyl-3-octadecylimidazolium p-toluenesulfonate

Ausbeute 91.3%

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeIn a 100 ml flask equipped with a stirrer, a condenser and a calcium chloride dryer tube
2. 2
   TemperaturAfter cooling the reaction mixture to room temperature
3. 3
   Sonstigeprecipitated crystals
4. 4
   Filtrationwere collected by filtration under reduced pressure
5. 5
   SonstigeThe resulting crystals were recrystallized from acetone

Vorschrift

In a 100 ml flask equipped with a stirrer, a condenser and a calcium chloride dryer tube were charged 3.7 g of 1-methylimidazole and 10.0 g of octadecyl p-toluenesulfonate, and the mixture was stirred at 120° C. for 5 hours. After cooling the reaction mixture to room temperature, precipitated crystals were collected by filtration under reduced pressure. The resulting crystals were recrystallized from acetone to obtain 10.9 g of the title compound. Melting point: 71° C.

Quelle