Reaktion #71580
ord-a167b60b59f440498a8198b5d77db73e
Reaktionsgleichung
Reagenzien
Keine
Reaktionsbedingungen
Temperatur
40°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1Temperaturthe reaction mixture is heated
- 2Temperaturto reflux at 110° C. for 1½ hour
Vorschrift
144.2 g of Octanoic Acid is charged at room temperature and heated to 40° C., then 154.64 g of Thionyl Chloride is added over a period of 1 hour and the reaction mixture is heated to reflux at 110° C. for 1½ hour to obtain crude Octanoyl Chloride.