Reaktion #71580

ord-a167b60b59f440498a8198b5d77db73e

Reagenzien

Keine

Reaktionsbedingungen

Temperatur
40°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Temperaturthe reaction mixture is heated
  2. 2
    Temperaturto reflux at 110° C. for 1½ hour

Vorschrift

144.2 g of Octanoic Acid is charged at room temperature and heated to 40° C., then 154.64 g of Thionyl Chloride is added over a period of 1 hour and the reaction mixture is heated to reflux at 110° C. for 1½ hour to obtain crude Octanoyl Chloride.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08536355B2uspto-grants-2013_09