Reaktion #71572

Reaktionsgleichung

tetrahydrothiophene

methyltrifluoromethane sulfonate

→

Methyl-Tetrahydrothiophene Triflate

Lösungsmittel

dichloromethane

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeAs a result, a white solid product in a salt form was obtained after about 5 minutes
2. 2
   FiltrationThe solid product was filtered
3. 3
   Sonstigedried for 1 hour in an oven at 50° C.
4. 4
   Sonstigeto obtain the following product

Vorschrift

11 mmol of tetrahydrothiophene was dissolved in 10 ml of dichloromethane at 0° C., and about 12 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture. As a result, a white solid product in a salt form was obtained after about 5 minutes. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

Quelle