Reaktion #710461
ord-e4ad890d40d44f70a28960b2754401a0
Reaktionsgleichung
2-amino-3-methyl 5-bromobenzoic acid methyl ester
N,N-diethyl ethylenediamine
→
N-diethylaminoethyl-2-amino-3-methyl-5-bromobenzamide
Ausbeute 84.2%
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Temperatur
78°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1Sonstigereacted for 4 hours
Vorschrift
To a 100 mL round-bottom flask, 0.1 mol of 2-amino-3-methyl 5-bromobenzoic acid methyl ester having the structural formula of VIII-2, 100 mL of ethanol, 0.3 mol of N,N-diethyl ethylenediamine were added, heated to 78° C. and reacted for 4 hours, after treatment 27.5 grams of N-diethylaminoethyl-2-amino-3-methyl-5-bromobenzamide having a structural formula of III-2 was obtained, and the yield was 84.2%;